Two transmission electron microscopes (JEOL 2100F, Topcon 002B) are in operation with a periphery comprising specimen stages for in-situ electron microscopy and electron tomography as well as a specimen preparation facility. The standard techniques of nanocharacterization are available such as high-resolution imaging, electron diffraction, electron energy-loss spectroscopy, and electron tomography. The expertise is focused on in-situ electron microscopy and electron tomography where the group\’s own research projects are carried out.
Microscopie Electronique en Transmission
Le personnel
Corinne BOUILLET
Ingénieure de Recherche (IR1) – CNRSIPCMS – Département Surfaces et Interfaces (DSI) 23 rue du Loess BP 43 Bureau : 0032 Strasbourg 67034 Téléphone: +33 (0)3 88 10 70 30Fax: +33 (0)3 88 10 72 49 Courriel: Site internet: page personnelle
Ovidiu ERSEN
Professeur des universités – UNISTRAIPCMS – Département Surfaces et Interfaces (DSI) 23 rue du Loess BP 43 Bureau : 1041 Strasbourg 667034 Téléphone: +33 (0)3 88 10 70 28Fax: +33 (0)3 88 10 72 49 Courriel: Site internet: page personnelle
Dris IHIAWAKRIM
Ingénieur d’Etudes (IE2) – CNRSIPCMS – Plateforme Microscopie électronique 23 rue du Loess BP 43 Bureau : 0031 Strasbourg 67034 Téléphone: +33 (0)3 88 10 70 15Fax: +33 (0)3 88 10 72 49 Courriel personnel: Site internet: page personnelle
Instrumentation
Transmission electron microscopes
– Jeol 2100F (200 kV, Cs-corrected condenser, imaging filter, EDX, biprism, 2 CCD cameras) – Topcon 002B (200 kV, EDX, CCD camera)
Specimen stages
– single and double tilt – tomography (+/- 80°) – heating (< 1000°C) – cooling (liq. N2) – STM Nanofactory
Specifications of the instrumentation
– image resolution in STEM: 0.11 nm – image resolution in TEM: 0.2 nm – energy resolution in EELS: 0.7 eV – tilt range for tomography: +/- 80° – specimen temperature range: -190 – 1000°C
Specimen preparation facilities
– mechanical grinding, cutting, dimpling etc. – ion milling – chemical preparation
Techniques
– scanning transmission electron microscopy STEM – in-situ electron microscopy – electron tomography – electron energy-loss spectroscopy EELS – electron diffraction – electron holography
Services Work
for other groups concentrates on (at present): – spintronics – inorganic materials – catalysis
Applications
– Independent research projects of the platform are carried out in the fields of: – carbon nanomaterials (graphene, nanotubes) – nanocomposites (carbon-metal nanoparticles) – atomic defects in nanomaterials – interfaces in nanomaterials – nanoparticles in catalysis
Education
Electron microscopy is now part of regular courses for the bachelor and master level in physics at the University of Strasbourg. Courses are also held for the PhD school (Ecole Doctorale de Physique) in Strasbourg. Several PhD students carry out their research dedicated to electron microscopy.